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Dissolve H-Glu-OtBu (7.7 kg, 1.1 eq) in DCM (54 L) at 20C, then add a solution of TMSA (11.3 kg) dissolved in DCM (7 L), then stir the reaction mixture for 1 hr at 40C
10.1016/j.ejphar.2018.07.031 12 alarY.zgrH.MaturI.YenilmezE
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