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Deep or intra-articular injection is a clinical procedure, not a home protocol

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Initiate appropriate supportive treatment according to the patient's clinical signs and symptoms

An ACQUITY UPLC BEH HILIC column (1.7 m, 2.1 150 mm, Waters) and a gradient mobile phase consisting of water with 50 mM ammonium acetate (phase A) and acetonitrile (phase B) were used for chromatographic separation