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All of them were kept at 4 C for several days without a noticeable change in the analytes content

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[0044] The cleaving in step 7) is performed with TFA:PhSMe:PhOMe:EDT:H 2 O:TIS:PhOH=8090:05:03:05:05:02:05(V:V), with TFA:PhSMe:PhOH:EDT:H 2 O=85:5:3:5:2 being preferred